May | ||||||
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29 | 30 | 1 | 2 | 3 | 4 | 5 |
6 | 7 | 8 | 9 | 10 | 11 | 12 |
13 | 14 | 15 | 16 | 17 | 18 | 19 |
20 | 21 | 22 | 23 | 24 | 25 | 26 |
27 | 28 | 29 | 30 | 31 | 1 | 2 |
June | ||||||
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27 | 28 | 29 | 30 | 31 | 1 | 2 |
3 | 4 | 5 | 6 | 7 | 8 | 9 |
10 | 11 | 12 | 13 | 14 | 15 | 16 |
17 | 18 | 19 | 20 | 21 | 22 | 23 |
24 | 25 | 26 | 27 | 28 | 29 | 30 |
July | ||||||
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1 | 2 | 3 | 4 | 5 | 6 | 7 |
8 | 9 | 10 | 11 | 12 | 13 | 14 |
15 | 16 | 17 | 18 | 19 | 20 | 21 |
22 | 23 | 24 | 25 | 26 | 27 | 28 |
29 | 30 | 31 | 1 | 2 | 3 | 4 |
August | ||||||
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29 | 30 | 31 | 1 | 2 | 3 | 4 |
5 | 6 | 7 | 8 | 9 | 10 | 11 |
12 | 13 | 14 | 15 | 16 | 17 | 18 |
19 | 20 | 21 | 22 | 23 | 24 | 25 |
26 | 27 | 28 | 29 | 30 | 31 | 1 |
September | ||||||
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26 | 27 | 28 | 29 | 30 | 31 | 1 |
2 | 3 | 4 | 5 | 6 | 7 | 8 |
9 | 10 | 11 | 12 | 13 | 14 | 15 |
16 | 17 | 18 | 19 | 20 | 21 | 22 |
23 | 24 | 25 | 26 | 27 | 28 | 29 |
30 | 1 | 2 | 3 | 4 | 5 | 6 |
October | ||||||
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30 | 1 | 2 | 3 | 4 | 5 | 6 |
7 | 8 | 9 | 10 | 11 | 12 | 13 |
14 | 15 | 16 | 17 | 18 | 19 | 20 |
21 | 22 | 23 | 24 | 25 | 26 | 27 |
28 | 29 | 30 | 31 |
Notebook
Welcome to our notebook!
Click on the calendar if you are curious to see what we did each week.
Week 21
Who worked: Simen, Linnea
Transformation
- E. coli (DH5a) transformed with pBAD
- Used LB media with ampicillin
Miniprep
- Miniprep of transformed cultures
- RESULT: concentrations of pBAD --> Sample 1: 52ng/ul, Sample 2: 54ng/ul
PCR
- PCR of pBAD, Sample 2 (from miniprep)
- Annealing temperatur: 64°C
- RESULT: No product on gel.Thinking of doing Gradient PCR to find right annealing temperature
Week 22
Who worked: Simen, Linnea
Gradient PCR
- Trying to find optimal PCR temperatures between 59°C - 69°C
- 8 samples made with different annealing temperatures from Sample 2, pBAD (made week 21)
- RESULT: Samples : 7 (68.3°C) and 8 (69°C) looked good on the gel.
Week 23
Restricted lab access
Week 24
Restricted lab access
Week 25
Who worked: Simen, Alec, Prabin
DpnI digestion
- Digestion of all gradient PCR products 1-8 (made Week 22)
- DNA was run on a gel after digestion with DpnI
- RESULT: concentration sample 7 (36.5ng/ul)
Gel Purification
- Purification of gel
Gibson assembly
- 3 gibson assemblies, putting pBAD together with each of our three genes: crtI, crtE and crtB
- Used the pBAD backbone from sample 7
- Had two controls, one with our pBAD vector from Sample 7, together with Gibson mix and the other one with only pBAD and water
Rxn 1 | Concentration | Amount Needed |
pBAD | 36.5ng/ul | 3ul |
CrtI | 28ng/ul | 3ul |
2xGibson mix | -------- | 6ul |
Rxn 2 | Concentration | Amount Needed |
pBAD | 36.5ng/ul | 3ul |
CrtE | 17ng/ul | 2ul |
2xGibson mix | -------- | 5ul |
Rxn 3 | Concentration | Amount Needed |
pBAD | 36.5ng/ul | 3ul |
CrtB | 47ng/ul | 1ul |
2xGibson mix | -------- | 4ul |
- RESULTS:
Making competent cells
RESULT: succesful
Transformation
- Transformation of crtB, crtE and crtI into DH5a
- RESULT: number of colonies --> crtB (14 colonies), crtE (5 colonies) and crtI (2 colonies)
Colony PCR
- Only sample 7 and 8 were done gel extractions on
Colony PCR
- Colony PCR with colonies from gibson assembly
- Petri dish with numbered grids was added colonies from the Gibson reaction
- Colonies with pBAD-crtB, pBAD-crtE and pBAD-crtI were added to plate in grid 1-14, 15-19 and 20-21, respectively
- Remaining cells, after colonies were added to grid, were done colony PCR on
Liquid culture
- Made liquid cultures of colonies: 7 and 14 (crtB), 15 and 19 (crtE) and 20 (crtI) for the next day
- Gave the samples new names. 7= crtB1, 14=crtB2, 15=crtE1, 19=crtE2, 20=crtI
Miniprep
- Miniprep preformed on inoculated samples from day before.
- RESULT: concentrations -- > crtB1 (121.2ng/ul), crtB2(118.9ng/ul), crtE1(144.5ng/ul), crtE2(125.4ng/ul), crtI(133.2ng/ul)
Sequencing
- crtB1, crtB2, crtI, crtE1 and crtE2 sent for sequencing
- RESULT: crtB1 and crtI had the correct sequence and were kept for SDS-PAGE (week 26), CrtE1 and E2 had faults in the sequence and were thrown away
Expression Test
- Made expression cultures of colonies crtE1 and 2, crtB1 and 2, and crtI
- Induction with 0.1% final concentration of Arabinose
- RESULT: the expression seemed to have been a failure, with no difference between the induced and the non-induced cultures. The expression test needs to be repeated. Next time the cultures should contain glucose? Also, does DH5a consume arabinose so that the expression won’t work unless we use another strain?
Week 26
Who worked: Simen, Alec, Marthe
Miniprep
- On colonies 16-18 (crtE)
Sequencing
- Miniprepped DNA from colonies 16-18 were send for sequencing
Week 27
Who worked: Bianca, Simen, Alec
Transformation
- Transformation of pBAD-crtI, pBAD-crtE and pBAD-crtB into DH5a cells
- RESULT: several colonies on plate
Preculture
- Made pre-cultures on crtI, crtE and crtB
Week 28
Who worked: Alec, Bianca
Cell Lysis
- Lysis of cells by sonication
SDS-PAGE
- Run proteins on SDS gel from crtI, crtE and crtB from previous week
Week 29
Who worked: Prabin, Linnea, Alec, Simen
Preculture
- Setting up new precultures to test crtE and crtI
Expression culture
- Making expression culture from preculture of crtE and crtI
- 0.2% Glucose, 100ug/ml ampicillin
- Two different concentrations of arabinose: 0.2% and 0,02%
- RESULT: crtE (OD600 = 0.7968), crtI (OD600 = 0.847)
Cell lysis
- Cell lysis of cells in expression culture by Sonication
SDS-PAGE
- SDS-PAGE of lysed cells after expression cultures
Expression test
- Expression test on crtI
Done glucose free, with 0.1ng/ml ampicillin
- Two different concentrations of arabinose: 0.2% and 0,02%
- Checked OD600 after 3 and 3.5hrs.
- RESULT: 3hrs (OD600 = 0.3359), 3.5hrs (OD600 = 0.5038)
Cell lysis
- Cell lysis of cells in expression culture by Sonication
SDS-PAGE
- The lysed cells were run on an SDS-gel
- The samples from the last expression test, were made dilutions on and run on a SDS-gel
- The dilutions were: 1x, 2x, 3x, 5x, 10x, 20x, 50x, 100x
Week 30
Who worked: Alec, Prabin
Preculture
- Precultures of crtE, crtI and crtB.
- Used low Glucose LB media
Expression test
- Made expression culture from preculture
Done with 0.1ng/ml ampicillin
- Five different concentrations of arabinose, 0.05%, 0.1%, 0.2%, 0.5% and 1%
- DEVIATION: Shaker stopped overnight
- RESULT: after 3.5hrs, 2% arabinose -- > crtB (OD600 = 0.872), crtE (OD600 = 0.913), crtI (OD600 = 0.867)
SDS-PAGE
- Making test gel for testing all samples from expression test
- RESULT: Something went wrong and the bands were barely visible on the gel. Will run SDS again without dilutions
SDS-PAGE
- SDS-gel with samples from expression test run without dilutions, only 2% arabinose samples.
Week 31
Lab closed due to building maintenance
Week 32
Who worked: Alec, Simen, Prabin
Preculture
- Preculture of crtE, crtB and crtI, with ampicillin
Expression Test
- Made expression culture from preculture
- Three different concentrations of arabinose, 0.5%, 1%, 2%
- RESULT: after 3hrs -- > crtB (OD600 = 0.5406), crtE (OD600 = 0.6145), crtI (OD600 = 0.6248).
after 24hrs -- > (see table for OD600)
% Arabinose | 0% | 0.5% | 1% | 2% |
crtE | 1.1 | 2.1 | 2.0 | 1.8 |
crtB | 2.6 | 2.1 | 2.2 | 1.9 |
crtI | 2.4 | 2.3 | 2.1 | 2.0 |
Week 33
Who worked: Marthe, Simen, Alec, Prabin
Colony PCR
- Colony PCR of colony 17 and 18 crtE and colony 1 and 2 crtB
- RESULT: Amplification was successful. crtE also had significant amplification of unspecific product
DpnI Digestion
- DpnI Digestion on DNA product from colony PCR
DNA Purification
- Purification of DNA product from DpnI digestion.
- Purification of product 2 (crtE) using the Monarch DNA Purification Protocol
- Purification of product 4 (crtB) using Mini Elute PCR Purification Kit
- RESULT: concentrations -- > crtE (3.3ng/ul), crtB (141.8ng/ul)
Cell Lysis
- Cell Lysis by sonication
Gradient PCR
- Setting up gradient PCR to improve yield of crtE
- Annealing temperatures from 60 - 70 °C
- RESULT: High temperatures had less unspecific binding. Next time, we will use 70°C annealing temperature for crtE
DpnI digestion
- DpnI digestion of crtE
DNA Purification
- DNA purification of crtE on gel with monarch kit
- RESULT: concentration -- > crtE (33ng/ul)
Gibson Assembly
- Gibson assembly of crtB into pBAD-crtE
Concentration | Amount Needed | |
pBAD-crtE | 33 ng/ul | 3 ul |
CrtB | 141 ng/ul | 1 ul |
2xGibson mix | -------- | 4 ul |
- RESULT: Multiple colonies. Will check them with colony PCR.
Week 34
Who worked: Marthe, Simen, Alec, Prabin
Colony PCR
- Colony PCR of 9 crtEB colonies
- RESULT: colony 6 looked good
Liquid culture
- Inoculation of colony 6, crtEB from grid plate after colony PCR
Gradient PCR
- Gradient PCR of crtEB and crtE
Mini-Prep
- Miniprep of inoculated culture from crtEB, colony 6
- RESULT: concentration -- > crtEB (98.5ng/ul)
NdeI Digestion
- NdeI digestion of crtEB and crtE after gradient PCR
PCR
- PCR of NdeI digested crtEB and crtE, as well as colonies 1-7 and 16-18 of crtEB from Gibson assembly
PCR
- Repeat last PCR
Transformation
- Transformation crtEB into DH5a
- RESULT: 24 colonies
Colony PCR
- Colony PCR of colonies from Transformation
- RESULT: none of the colonies had the insert
Week 35
Who worked: Alec, Simen , Kristin, Linnea
PCR
- Amplification of crtB and crtE
DpnI digestion
- DpnI digestion of PCR product
Gel purification
- Gel purification on PCR product
Purification of crtE (Gene JETgel extraction kit) and crtB (PCR purification Kit)
-RESULT: concentrations -- > crtE vector yield (15.9ng/ul), crtB (195ng/ul)
Gibson assembly
- Gibson assembly of crtB into the pBAD-crtE vector
Concentration | Amount Needed | |
pBAD-crtE | 15 ng/ul | 7.0 ul |
CrtB | 195ng/ul | 0.6 ul |
2xGibson mix | -------- | 7.6 ul |
- RESULT: The Gibson assembly was successful!
Gel purification
- Gel purification with monarch protocol
-RESULT: crtB concentration 65.0ng/ul
PCR purification
- Purification of sample 5, crtB from PCR (from week 33)
- RESULT: concentration 195ng/ul of crtB
Transformation
- Transformation of the crtEB , from the Gibson assembly, into DH5a cells
Colony PCR
- Colony PCR of colonies from transformation
- Remark: 0.5ul was used instead of 0.25ul.
- Leftovers from recovery was plated on Amp-LB plate.
Mini prep
- Miniprep of pBAD-crtEB product, colony 1, from colony PCR.
Sequencing
- Miniprep product from colony 1 (pBAD-crtEB) sent for sequencing.
Colony PCR
- Checking 8 colonies from the transformation.
-------------------------HQ-part-------------------------
Dissolve DNA pellet in water
- Dissolve pellet, from the ordered pBAD-crtEBI construct, in water
Transformation
- Transformation of crtEBI-HQ into DH5a cells
- REMARK: HEatshock was too long
- RESULT: successful transformation
Pre-culture
- Pre-culture of colonies from the transformation
Mini-Prep
- Mini-prep of DNA from pre-culture
- RESULT: pink/red pellet. Concentration 87.4ng/ul
Week 36
Who worked: Kristin, Marthe, Simen, Linnea, Alec
PCR
- 3x different PCR reaction
- Two samples per reaction, 6 samples in total.
Rxn 1: crtEB, Rxn 2: crtI insert, Rxn 3: pBAD vector.
Gel purification
- The products from the PCR are all run on a gel and purified.
RESULT: crtEB vector (7.7ng/ul), crtI insert (46.2ng/ul), pBAD vector (21.0 ng/ul)
Gradient PCR
- Gradient PCR done on pBAD-crtEB vector
- Annealing temperature set from 59°C – 69°C for samples.
DpnI Digestion
- DpnI digestion of gel purified product.
- Done on 37°C for 1h
Gibson Assembly
- Gibson assembly of crtI insert into vector with crtEB
1st TRY | Concentration | Amount Needed |
CrtEB | 7.7 ng/ul | 14 ul |
CrtI | 46.2 ng/ul | 2 ul |
2xGibson mix | -------- | 16 ul |
- RESULT: Assembly not successful
Transformation
- Transformation of product from Gibson assembly, pBAD-crtEBI, into DH5a
- RESULT: Colonies on plate
Colony PCR
- Colony PCR of 32 colonies from Transformation
Grid plate made for all colonies in the PCR reaction
Inoculation Of Colonies
- Inoculation of colonies; 2, 6 and 10 from grid plate made with colony PCR
Miniprep
- Miniprep of inoculated colonies
NdeI Digestion
- NdeI digestion of miniprepped colonies: 2, 6 and 10.
- Digest run on gel
Gradient PCR
- Gradient PCR of crtEB
- Annealing temperature set from 59°C – 69°C for samples.
------------------------------HQ-Part------------------------------
PCR
- PCR of the mini prepped product (week 35)
Gel purification
- Run the PCR product on a gel and do gel purification
- RESULT: concentration -- > crtEBI-HQ (30.5ng/ul)
Gibson Assembly
- Cloning crtEBI into our own pBAD backbone, trying to fix leaky expression.
Concentration | Amount Needed | |
CrtEBI-HQ | 30.5 ng/ul | 9ul |
pBAD | 27.0 ng/ul | 5 ul |
2xGibson mix | -------- | 14 ul |
Transformation
- Transform product from Gibson assembly into DH5a cells
- DEVIATION: used 15ul Gibson solution, instead of 14 (supposed to have 1:1 relation)
- RESULT: no colonies
Week 37
Who worked: Marthe, Simen, Kristin, Linnea, Alec
DpnI Digestion
- DpnI digestion of amplified crtEB. (From fist PCR, preformed week 36)
PCR Purification
- PCR purification of pBAD and crtI ()
Gibson Assembly
- Gibson assembly of crtI and crtEB into pBAD
2nd TRY | Concentration | Amount Needed |
CrtEB | 38.6 ng/ul | 2.8 ul |
CrtI | 144.2 ng/ul | 0.64 ul |
2xGibson mix | -------- | 3.4 ul |
- RESULT: No colonies on plate
Gibson Assembly
- Assembly of crtEB and crtI into pBAD vector
- Making reaction with 1:3 ratio between number of inserts and backbones
3rd TRY | Concentration | Amount Needed |
CrtEB | 38.6 ng/ul | 2.6 ul |
CrtI | 144.2 ng/ul | 7.2 ul |
2xGibson mix | -------- | 9.8 ul |
- RESULT: No colonies on plate
PCR
- PCR of crtEB and crtI
- The annealing temperatures were: 69°C for crtEB and 63°C for crtI
- The buffers were : GC for crtEB and HF for crtI
DpnI Digestion
- Digestion of all PCR products 1-8
Gel Purification
- Purify products from the DpnI digestion
Gibson Assembly
- Assembly og crtEB together with crtI pBAD
- Making reactions with a 1:3 ratio between number of inserts and backbones
4th TRY | Concentration | Amount Needed |
CrtEB | 17 ng/ul | 5.9 ul |
CrtI | 19 ng/ul | 4.6 ul |
2xGibson mix | -------- | 10.5 ul |
- RESULT: many colonies
Colony PCR
- PCR of 16 colonies from last gibson assembly
- Used crtEB vector as control
- Colonies boiled for 10min, 98°C
Colony PCR
- Re-run of PCR of all colonies except colony 15
- 2min elongation time, on all colonies except nr. 15
- RESULT: None of the grid plate colonies grew up
------------------------------HQ-Part------------------------------
PCR Purification
- Purification of PCR product form first PCR, week 36
Gibson Assembly
- Cloning crtEBI into our own pBAD backbone, trying to fix leaky expression
1st TRY | Concentration | Amount Needed |
CrtEBI-HQ | 49.3 ng/ul | 5.6 ul |
pBAD | 41.9 ng/ul | 3.2 ul |
2xGibson mix | -------- | 8.8 ul |
- RESULTAT: No colonies on plate
Gibson Assembly
- Cloning crtEBI into our own pBAD backbone, try nr. 2
- Making reaction with 1:3 ratio between number of inserts and backbone
2nd TRY | Concentration | Amount Needed |
CrtEBI-HQ | 49.3 ng/ul | 6.8 ul |
pBAD | 41.9 ng/ul | 2.4 ul |
2xGibson mix | -------- | 9.2 ul |
DEVIATION:
- RESULTAT: No colonies on plate
PCR
- PCR of crtEBI-HQ and pBAD
- Annealing temperature was set to 63°C
DpnI Digestion
- DpnI digestion of all PCR products 1-8, from last PCR
Gel Purification
- Purification of products from DpnI digestion
Gibson Assembly
- Cloning crtEBI into our own pBAD backbone, try nr. 2
- Making reaction with 1:3 ratio between number of inserts and backbone
3rd try | Concentration | Amount Needed |
CrtEBI-HQ | 47.2 ng/ul | 5.6 ul |
pBAD | 19.2 ng/ul | 5.2 ul |
2xGibson mix | -------- | 10.8 ul |
- RESULT: Many colonies on plate
Colony PCR
- PCR of 16 colonies from Gibson cloning, try nr. 3
- Used pBAD vector as control
- Colonies boiled for 10 min, 98°C
-
Week 38
Who worked: Simen
Gibson Assembly
- Gibson assembly repeated again (from week 37), 5th try.
- Use plates with arabinose
5th TRY | Concentration | Amount Needed |
CrtEB | 17 ng/ul | 5.9 ul |
CrtI | 19 ng/ul | 4.6 ul |
2xGibson mix | -------- | 10.5 ul |
- RESULT: No colonies. We think the problem has to do with the DNA concentration. The DNA concentration has to be improved.
Colony PCR
- PCR of colonies from 4th try of gibson assembly
Gel Purification
-RESULT: crtEB (16.4 ng/ul), crtI (40.4 ng/ul)
PCR
-Re-do of PCR
- PCR of crtI and crtEB
- GC buffer on crtEB and HF buffer on crtI
PCR Purification
- Purification of PCR products
- RESULTS: crtEB (108.4 ng/ul), crtI (206.55 ng/ul)
Gibson Assembly
- Making reaction with a 1:3 ratio between number of inserts and backbones
Concentration | Amount Needed | |
CrtEB | ng/ul | ul |
CrtI | ng/ul | ul |
2xGibson mix | -------- | ul |
- RESULTS: colonies on gel!
------------------------------HQ-Part------------------------------
PCR
- Re-do of first PCR, from week 37
- PCR of crtEBI-HQ and pBAD
PCR Purification
- Purification of PCR products
- RESULT: crtEBI-HQ (108.4 ng/ul), pBAD (206.6ng/ul)
Gibson Assembly
- Insetion of crtEBI into pBAD
- Making reaction with 1:5 ratio between number of inserts and backbone
Concentration | Amount Needed | |
CrtEBI-HQ | ng/ul | ul |
pBAD | ng/ul | ul |
2xGibson mix | -------- | ul |
- RESULT:
Week 39
Who worked: Simen, Alec, Prabin, Linnea
Colony PCR
- PCR of colonies from last Gibson assembly, (week 38)
Expression Test
- Expression test of cultures 4 and 5 from colony PCR
- 2% Arabinose, 4hrs
Mini-Prep
- Made liquid cultures of colony 5 -> miniprep -> send for sequencing
Colony PCR
- Colony PCR of pBAD-crtE, amplifying pBAD vector – want to make an empty pBAD vector as control
- RESULT: No pBAD amplification? No growth on grid plate?
------------------------------HQ-Part------------------------------
Colony PCR
- PCR of colonies from last gibson assembly, week 38
Expression test
- Expression test of colonies 1, 7, 8 and 11
- 2% arabinose, 4hrs
- NOTE: out of arabinose, only colonies 1 and 7 induced
- RESULT: For both 1 and 7, the induced cultures had a brighter red colour than the un-induced cultures
Mini-Prep
- Made liquid cultures of colonies 1 and 7 --> mini prep
Sequencing
- DNA from mini-prepped colonies send for sequencing
Colony PCR
- for making pBAD control
- This is the same as what was done for our own sample, not from the HQ
Week 40
Who worked: Simen, Prabin, Marthe, Kristin, Alec
Transformation
- Transformation of cells with empty pBAD vector (to be used as control)
Gibson Assembly
- Making reaction with 1:3 ratio between number of inserts and backbones
Concentration | Amount Needed | |
CrtEB | 108.4 ng/ul | 1 ul |
CrtI | 100 ng/ul | 0.84 ul |
2xGibson mix | -------- | 1.84 ul |
- RESULT: 23 colonies on gel
Colony PCR
- Colony PCR of colonies from transformation.
- RESULT: no colonies with crtEBI -> the Gibson was a failure
Sequencing
- DNA from colonies 1, 5 and 7 sent for sequencing
Gibson Assembly
- Repeating gibson assembly
PCR
- PCR of colony 5. pBAD and crtEB as control
Transformation result
- looking at result from transformation
Mini-Prep
- Mini-prep of colony 5
- RESULT: concentration -- > colony 5 (169.9ng/ul)
Freezer cultures
- Made freezer cultures of samples with empty pBAD vector
Preculture
- Preculture of colony 5 and pBAD(empty vector), for expression test
Expression test
t | Colony 5 (A600) | Colony 5 (A450) | pBAD (A600) | pBAD (A450) |
0 | 0.029 | ---- | 0.029 | |
30 | 0.036 | ---- | 0.034 | |
60 | 0.045 | ---- | 0.052 | |
90 | 0.075 | ---- | 0.048 | |
120 | 0.134 | ---- | 0.181 | |
150 | 0.186 | ---- | 0.228 | |
180 | 0.305 | ---- | 0.387 | |
195 | 0.377 | 0.532 | 0.445 | 0.605 |
210 | 0.479 | 0.644 | 0.472 | 0.624 |
225 | 0.453 | 0.603 | 0.539 | 0.705 |
240 | 0.504 | 0.695 | 0.59 | 0.788 |
255 | 0.513 | 0.785 | 0.66 | 0.858 |
270 | 0.670 | 0.884 | 0.727 | 0.932 |
285 | 0.765 | 0.956 | 0.793 | 0.983 |
300 | 0.842 | 1.036 | 0.841 | 1.027 |
315 | 0.892 | 1.083 | 0.882 | 1.062 |
330 | 0.97 | 1.14 | 0.901 | 1.089 |
345 | 1.019 | 1.187 | 0.939 | 1.118 |
360 | 1.064 | 1.227 | 0.96 | 1.137 |
375 | 1.091 | 1.258 | 0.974 | 1.158 |
390 | 1.111 | 1.282 | 0.979 | 1.167 |
405 | 1.136 | 1.301 | 0.994 | 1.178 |
------------------------------HQ-Part------------------------------
Mini-Prep
- Mini-prep of colonies 1 and 7
- RESULT: concentration -- > colony 1 (212.7ng/ul), colony 7 (139.5ng/ul)
Freezer cultures
- Made freezer cultures of colonies 1, 7, 8 (original HQ sample)
Preculture
- Preculture of colony 1 and 8, for expression test
Expression test
t | Colony 1 (A600) | Colony 1 (A450) | Colony 8 (A600) | Colony 8 (A450) |
0 | 0.028 | ---- | 0.016 | ---- |
30 | 0.033 | ---- | 0.016 | ---- |
60 | 0.042 | ---- | 0.027 | ---- |
90 | 0.079 | ---- | 0.056 | ---- |
120 | 0.937 | ---- | 0.108 | ---- |
150 | 0.175 | ---- | 0.142 | ---- |
180 | 0.297 | ---- | 0.244 | ---- |
195 | 0.375 | 0518 | 0.306 | 0.436 |
210 | 0.474 | 0.626 | 0.397 | 0.540 |
225 | 0.440 | 0.599 | 0.503 | 0.650 |
240 | 0.490 | 0.674 | 0.477 | 0.658 |
255 | 0.560 | 0.755 | 0.553 | 0.735 |
270 | 0.642 | 0.843 | 0.620 | 0.826 |
285 | 0.720 | 0.917 | 0.705 | 0.895 |
300 | 0.784 | 0.982 | 0.766 | 0.968 |
315 | 0.826 | 1.026 | 0.833 | 1.016 |
330 | 0.888 | 1.076 | 0.879 | 1.066 |
345 | 0.920 | 1.111 | 0.922 | 1.105 |
360 | 0.952 | 1.136 | 0.947 | 1.129 |
375 | 0.972 | 1.158 | 0.962 | 1.151 |
390 | 0.986 | 1.176 | 0.985 | 1.171 |
405 | 1.005 | 1.188 | 0.994 | 1.185 |
Week 41
Who worked: Simen, Alec, Kristin, Marthe, Prabin, Bianca
Colony PCR
- Colony PCR for crtEBI
- RESULT: None of the colonies have the insert
Preculture
- Preculture of crtEBI construct in DH5a and BL21 cells, the HQ-part (Bba_274100) in BL21 cells, BL21 cells with the pBAD vector (no insert)
Expression culture
- Expression culture of precultures
- 16hrs, 2% arabinose
- RESULT: Successful recovery of lycopene containing cells from the HQ-part (Bba_K274100), our cells failed to produce lycopene
Sequencing
- Sequencing of our crtEBI construct
Solar Cell Prototyping
- Made a prototype solar cell from the induced cultures of BL21 cells with the HQ part (Bba_K274100) in the pBAD vector
- RESULT: Titanium dioxide layer cracked and flaked, very poor voltage produced.
Week 42
Who worked: Simen, Alec, Prabin
Preculture
- Preculture of crtEBI and pBAD vector (no insert) in DH5a cells and in BL21 cells
Expression test
- Expression culture of the 4 different precultures
- Incubation for 40hrs, 2% arabinose
- RESULT: Successful recovery of lycopene containing cells. Found out our construct produces more lycopene in DH5a than in BL21
SDS-PAGE
- SDS-PAGE of last expression culture, to ensure that crtE, I and B are all expressed when appropriate
- RESULT: Gel was inconclusive but suggests only small levels of CrtE, CrtB, and CrtI expression.
Lycopene extraction
- Lycopene extraction of the cultures above
- RESULT: Our construct, crtEBI, produces measurable amounts of lycopene, but not as much of the HQ part we ordered for characterization.
Solar Cell Prototyping
- Made a prototype solar cell from the induced cultures of BL21 cells with the pBAD vector (no insert), our EBI construct in DH5a cells, BL21 cells with the HQ part (Bba_K274100) in the pBAD vector
- RESULT: Final results were promising: 20mV more was produced in light conditions than in dark conditions when the panel was made with our crtEBI construct, whereas the difference was 40mV when the Bba_K274100 cells were used in the cell. However, the pBAD cells flaked far too much to be usable in a cell, no amperage was detected and voltage decreased very slowly after removal of light source. It also produced voltage in natural light conditions (through a window on a cloudy day).